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101.
102.
采用微波消解-原子荧光法对广东竹丝鸡肉中有毒有害元素砷的含量进行抽样检测分析。结果表明:该方法检出限为0.067μg/L,回收率为95.7%~101.2%;竹丝鸡肉中砷的检出率为100%,平均残留量为0.041 mg/kg,符合我国无公害畜禽肉中砷的限量标准,并达到了我国绿色食品中砷限量标准。 相似文献
103.
采用丙酮震荡提取样品,在水解衍生的步骤中创造性地使用试管加入吡啶盐酸盐,于220℃的烘箱里水解1.5 h,经过处理后使用气相色谱ECD进行测定。结果表明:该方法的线性范围为0.005~0.500 ng,相关系数为0.999 9;对香蕉、绿橙、花牛苹果、青苹果、猕猴桃、砀山梨6种空白基质分别进行了0.01、0.10、1.00 mg/kg 3个水平加标,其回收率为81.0%~106.4%,相对标准偏差(RSD,n=5)为0.3%~5.7%;该方法的最低检出限为0.01 mg/kg,并且烘箱水解的新方法操作简便 相似文献
104.
《Communications in Soil Science and Plant Analysis》2012,43(17-18):2479-2503
Abstract As a means of economic disposal and to reduce need for chemical fertilizer, waste generated from swine production is often applied to agricultural land. However, there remain many environmental concerns about this practice. Two such concerns, contribution to the greenhouse effect and stratospheric ozone depletion by gases emitted from waste‐amended soils, have not been thoroughly investigated. An intact core study at Auburn University (32 36′N, 85 36′W) was conducted to determine the source‐sink relationship of three greenhouse gases in three Alabama soils (Black Belt, Coastal Plain, and Appalachian Plateau regions) amended with swine waste effluent. Soil cores were arranged in a completely random design, and treatments used for each soil type consisted of a control, a swine effluent amendment (112 kg N ha?1), and an ammonium nitrate (NH4NO3) fertilizer amendment (112 kg N ha?1). During a 2‐year period, a closed‐chamber technique was used to determine rates of emission of nitrous oxide (N2O)–nitrogen (N), carbon dioxide (CO2)–carbon (C), and methane (CH4)–C from the soil surface. Gas probes inserted into the soil cores were used to determine concentrations of N2O‐N and CO2‐C from depths of 5, 15, and 25 cm. Soil water was collected from each depth using microlysimeters at the time of gas collection to determine soil‐solution N status. Application of swine effluent had an immediate effect on emissions of N2O‐N, CO2‐C, and CH4‐C from all soil textures. However, greatest cumulative emissions and highest peak rates of emission of all three trace gases, directly following effluent applications, were most commonly observed from sandier textured Coastal Plain and Appalachian Plateau soils, as compared to heavier textured Black Belt soil. When considering greenhouse gas emission potential, soil type should be a determining factor for selection of swine effluent waste disposal sites in Alabama. 相似文献
105.
106.
研究了用3种大口径毛细管柱分析由有机磷杀虫剂组成的“难分离有机磷对”。HP-1大口径毛细管柱只能分离由甲基对硫磷和其它有机磷杀虫剂组成的“有机磷对”;QF-1大口径毛细管柱能够分离部分“有机磷对”;阿皮松L固定液大口径毛细管柱能完全分离马拉硫磷和水胺硫磷组成的“有机磷对”。 相似文献
107.
108.
涩宁兰输气管道工程进度控制 总被引:1,自引:0,他引:1
运用项目工程的控制理论,结合国内管道工程建设的经验,创建了涩宁兰管道工程建设管理模式,从对材料的采办、发放、现场调拔到对进度数据统计分析、预测及计划执行情况进行分析,及时、合理地调配资源,确保月计划的完成,以实现工期控制目标。 相似文献
109.
本实验建立了饲料中有机氯农药(OCPs)残留的气相色谱-微池电子捕获检测器(GC-μECD)分析方法。试样经丙酮提取,硅胶层析柱净化后,用GC-μECD测定其中农药残留量。有机氯农药浓度在5.00~500.00ng/mLp,p’-DDD相关系数除为0.9960外,其余均大于0.998,线性关系良好;检测限除o,p’-DDT和p,p’-DDT为10μg/kg外,其余农药为5μg/kg;添加有机氯农药50μg/kg水平时回收率为77.1%~113.4%,添加200μg/kg时回收率为75.8%~107.3%;相对标准偏差为2.3%~11.1%。本方法对饲料中有机氯农药残留分析结果准确可靠。 相似文献
110.
Voluntary intake of silages in dairy cows depending on chemical composition and in vitro gas production characteristics 总被引:1,自引:0,他引:1
A study was conducted to investigate the possibilities to develop models for predicting the relative silage dry matter intake (SDMI) in dairy cows utilising information on chemical composition and in vitro gas production (GP) kinetics of silages. In five experiments, each with an average of 38 lactating dairy cows, SDMI was recorded for 15 grass silages made from primary growth and regrowth swards of timothy (Phleum pratense L.). The silages were characterised by chemical analysis and by utilising an automated in vitro GP recording technique with end point measurements of substrate residues. The silage samples were analysed both as dried and wet samples to evaluate the effects of sample preparation techniques on GP kinetics and their relations to SDMI. Relationships between feed variables and SDMI were investigated utilising simple linear and multiple regression. The wet silage samples had higher cumulative GP and different GP curves compared to the dried samples. The linear relationships between, GP variables, harvest number (first or second cut) of the grass, chemical characteristics of the silages and the relative SDMI show that the GP technique is a powerful tool to detect silage quality. By using the parameters from the dried samples the multiple regression analysis resulted in a relationship, relative SDMI (kg per 100 kg live weight (LW)) per day = 0.071 + 0.0029 × NDFD − 0.266 × C (R2 = 0.82, S.D. = 0.06). NDFD is the degradability of the neutral detergent fibre (NDF) (g/kg NDF) and C is the variable that regulates the switching characteristics of the GP profiles. By using the wet silage samples the multiple relationship did not include any GP variable; relative SDMI (kg per 100 kg LW per day) = 1.86 − 0.008 × acetic acid (g/kg DM) + 0.024 × ethanol (g/kg DM) (R2 = 0.62, S.D. = 0.08). The results from the regression analysis and the experience of the laborious sample preparation technique for wet samples, give the conclusion that dried silage samples are recommended for determining feed characteristics using the GP technique in intake studies. 相似文献